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Closely follows an actual structural determination. After some introductory material on the nature of x-rays, the diffraction process, and the internal geometry of crystals, the selection and preparation of a crystal are considered. Techniques of measuring raw x-ray data are covered, plus their reduction into a useable form. The second part discusses both traditional and novel methods of solving the ``phase'' problem, the principal difficulty in x-ray structure determination. The third part considers how to extract the most information from the data and how to evaluate its reliability. Finally, there is a discussion of sources of error in practice and interpretation.
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X-Ray Structure Determination, George H. Stout
- Langue
- Année de publication
- 1989
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- (rigide)
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- Titre
- X-Ray Structure Determination
- Sous-titre
- A Practical Guide, 2nd Edition
- Langue
- Anglais
- Auteurs
- George H. Stout
- Éditeur
- Wiley-Interscience
- Publié
- 1989
- Format
- rigide
- Pages
- 480
- ISBN10
- 0471607118
- ISBN13
- 9780471607113
- Séries
- Mots clés
- Science, Technologie, Physique, Chimie, Théories scientifiques, Chimie physique, Cristallographie
- Description
- Closely follows an actual structural determination. After some introductory material on the nature of x-rays, the diffraction process, and the internal geometry of crystals, the selection and preparation of a crystal are considered. Techniques of measuring raw x-ray data are covered, plus their reduction into a useable form. The second part discusses both traditional and novel methods of solving the ``phase'' problem, the principal difficulty in x-ray structure determination. The third part considers how to extract the most information from the data and how to evaluate its reliability. Finally, there is a discussion of sources of error in practice and interpretation.